1,3,2-Dioxaborolane-2-propanamine, 4,4,5,5-tetramethyl- synthesis

1synthesis methods

Product Name:1,3,2-Dioxaborolane-2-propanamine, 4,4,5,5-tetramethyl-
CAS Number:144266-60-4
Molecular formula:C9H20BNO2
Molecular Weight:185.07

2-(3-azidopropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

144266-69-3
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1,3,2-Dioxaborolane-2-propanamine, 4,4,5,5-tetramethyl-

144266-60-4
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Yield:144266-60-4 88%

Reaction Conditions:

with palladium on activated charcoal;hydrogen in ethanol;4 atm H2, 18 h, room temp., 10% Pd on charcoal; filtration, solvent removal (reduced pressure), washing (ether);

References:

Jego, J.M.;Carboni, B.;Vaultier, M. [Journal of Organometallic Chemistry,1992,vol. 435,# 1.2,p. 1 - 8]