Carbamic acid, N-[(4-bromo-2-hydroxyphenyl)methyl]-N-(2-hydroxyethyl)-, 1,1-dimethylethyl ester synthesis

1synthesis methods

Product Name:Carbamic acid, N-[(4-bromo-2-hydroxyphenyl)methyl]-N-(2-hydroxyethyl)-, 1,1-dimethylethyl ester
CAS Number:1445903-00-3
Molecular formula:C14H20BrNO4
Molecular Weight:346.22

22532-62-3 Synthesis

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Carbamic acid, N-[(4-bromo-2-hydroxyphenyl)methyl]-N-(2-hydroxyethyl)-, 1,1-dimethylethyl ester

1445903-00-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: methanol; sodium tetrahydroborate / tetrahydrofuran / 2 h / 40 °C
2: sodium hydrogencarbonate / water; ethyl acetate / 16 h / 20 °C

References:

WO2013/92941,2013,A1