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Propanal, 2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2-methyl- synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 50 percent / NaH / tetrahydrofuran / 3 h
2: DMSO; oxalyl chloride; triethylamine / CH2Cl2 / -78 - 20 °C

References:

Liu, Xuan;West [Chemical Communications,2006,# 48,p. 5036 - 5038]