3-(2-PHENYLACETYL)-(4R)-(PHENYLMETHYL)-2-OXAZOLIDINONE synthesis

1synthesis methods

Product Name:3-(2-PHENYLACETYL)-(4R)-(PHENYLMETHYL)-2-OXAZOLIDINONE
CAS Number:144838-82-4
Molecular formula:C18H17NO3
Molecular Weight:295.33

90719-32-7
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Benzeneacetic acid, anhydride with 2,2-dimethylpropanoic acid

864658-42-4
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3-(2-PHENYLACETYL)-(4R)-(PHENYLMETHYL)-2-OXAZOLIDINONE

144838-82-4
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$249.00/1g

Yield:144838-82-4 3.6 g

Reaction Conditions:

Stage #1: (S)-4-Benzyl-2-oxazolidinonewith n-butyllithium in tetrahydrofuran;hexane;
Stage #2: 2,2-dimethylpropanoicphenylacetic anhydride in tetrahydrofuran;diethyl ether;hexane at -78 - 0; for 0.75 h;

References:

Lu;Schiller [Synthesis,2001,# 11,p. 1639 - 1644]