ChemicalBook CAS DataBase List 1H-Indole-2-carboxylic acid, 4,6-dichloro-, Methyl ester

1H-Indole-2-carboxylic acid, 4,6-dichloro-, Methyl ester synthesis

1synthesis methods

Product Name:1H-Indole-2-carboxylic acid, 4,6-dichloro-, Methyl ester
CAS Number:144989-28-6
Molecular formula:C10H7Cl2NO2
Molecular Weight:244.07

2-Propenoic acid, 2-azido-3-(2,4-dichlorophenyl)-, methyl ester

1253935-19-1
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1H-Indole-2-carboxylic acid, 4,6-dichloro-, Methyl ester

144989-28-6
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Yield:144989-28-6 85%

Reaction Conditions:

with 5,10,15,20-tetrakis(pentafluorophenyl)-21H,23H-porphyrin iron(III) chloride in 1,2-dichloro-ethane; for 48 h;Molecular sieve;Reflux;Inert atmosphere;

References:

Liu, Yungen;Wei, Jinhu;Che, Chi-Ming [Chemical Communications,2010,vol. 46,# 37,p. 6926 - 6928] Location in patent:supporting information; experimental part