ChemicalBook CAS DataBase List 2-(3-(but-3-yn-1-yl)-3H-diazirin-3-yl)ethan-1-amine

2-(3-(but-3-yn-1-yl)-3H-diazirin-3-yl)ethan-1-amine synthesis

6synthesis methods

Product Name:2-(3-(but-3-yn-1-yl)-3H-diazirin-3-yl)ethan-1-amine
CAS Number:1450752-97-2
Molecular formula:C7H11N3
Molecular Weight:137.18

2-(3-But-3-ynyl-3H-diazirin-3-yl)-ethanol

1450754-41-2
64 suppliers
$65.00/5mg

2-(3-(but-3-yn-1-yl)-3H-diazirin-3-yl)ethan-1-amine

1450752-97-2
66 suppliers
$145.00/5mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: pyridine; dmap; triethylamine / dichloromethane / 0 - 20 °C
2: sodium azide / N,N-dimethyl-formamide / 70 °C
3: triphenylphosphine / tetrahydrofuran; water / 24 h

References:

He, Dan;Xie, Xiao;Yang, Fan;Zhang, Heng;Su, Haomiao;Ge, Yun;Song, Haiping;Chen, Peng R. [Angewandte Chemie - International Edition,2017,vol. 56,# 46,p. 14521 - 14525][Angew. Chem.,2017,vol. 129,p. 14713 - 14717,5]

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