2-(2-((4-bromophenyl)amino)-2-oxoethoxy)-N-(2-(methyl(phenyl)amino)-2-oxoethyl)benzamide synthesis
- Product Name:2-(2-((4-bromophenyl)amino)-2-oxoethoxy)-N-(2-(methyl(phenyl)amino)-2-oxoethyl)benzamide
- CAS Number:1462267-08-8
- Molecular formula:C24H22BrN3O4
- Molecular Weight:496.35
106-40-1
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 16 h / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C
3: potassium hydroxide; water / methanol; tetrahydrofuran / 16 h / 20 °C
4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1 h / 0 - 20 °C
5: triethylamine / dichloromethane / 16 h
References:
THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY, DEPARTMENT OF HEALTH AND HUMAN SERVICES;THE UNIVERSITY OF KANSAS;MARUGAN, Juan, Jose;ZHENG, Wei;PATNAIK, Samarjit;SOUTHALL, Noel;SIDRANSKY, Ellen;GOLDIN, Ehud;WESTBROEK, Wendy;AFLAKI, Elma;ROGERS, Steven, Andrew;SCHOENEN, Frank, John WO2013/148333, 2013, A1
2564-02-5
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1462267-08-8
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949969-59-9
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1462267-08-8
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