1(2H)-Isoquinolinone, 8-(dimethylamino)-3,4-dihydro- synthesis

1synthesis methods

Product Name:1(2H)-Isoquinolinone, 8-(dimethylamino)-3,4-dihydro-
CAS Number:1462328-70-6
Molecular formula:C11H14N2O
Molecular Weight:190.24

619-22-7
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1(2H)-Isoquinolinone, 8-(dimethylamino)-3,4-dihydro-

1462328-70-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: pyridine; piperidine
2: sodium azide; chloroformic acid ethyl ester; triethylamine / acetone
3: toluene / 110 °C
4: aluminum (III) chloride / dichloromethane / 25 °C

References:

Hong, Jun Bae;Davidson, James P.;Jin, Qingwu;Lee, Gary R.;Matchett, Michael;O'Brien, Erin;Welch, Michael;Bingenheimer, Bill;Sarma, Keshab [Organic Process Research and Development,2014,vol. 18,# 1,p. 228 - 238]