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ChemicalBook CAS DataBase List 1,2-Bis(diphenylphosphino)ethane nickel(II) chloride

1,2-Bis(diphenylphosphino)ethane nickel(II) chloride synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: oxalyl dichloride / dichloromethane / 1 h / 20 °C / Schlenk technique; Inert atmosphere; Sealed tube
2: hexachlorodisilane / dichloromethane-d2 / 0.08 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox
3: dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Glovebox

References:

Kapu?niak, ?ukasz;Plessow, Philipp N.;Trzybiński, Damian;Wo?niak, Krzysztof;Hofmann, Peter;Jolly, Phillip Iain [Organometallics,2021,vol. 40,# 6,p. 693 - 701]

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