2-Oxazolidinone, 5-(aminomethyl)-3-(4-methoxyphenyl)- synthesis

3synthesis methods

Product Name:2-Oxazolidinone, 5-(aminomethyl)-3-(4-methoxyphenyl)-
CAS Number:148915-85-9
Molecular formula:C11H14N2O3
Molecular Weight:222.24

3-[(4-methoxyphenyl)amino]-1,2-Propanediol

121082-77-7
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2-Oxazolidinone, 5-(aminomethyl)-3-(4-methoxyphenyl)-

148915-85-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 83 percent / sodium methoxide / toluene; methanol / 3 h / 105 °C
2: pyridine / 0 - 5 °C
3: sodium azide / dimethylformamide / 12 h / 40 °C
4: H₂ / 10percent Pd/C / methanol; ethyl acetate / 5 h / 760 Torr

References:

Gates, Kent S.;Silverman, Richard B. [Journal of the American Chemical Society,1990,vol. 112,# 25,p. 9364 - 9372]

42902-32-9 Synthesis

5-HYDROXYMETHYL-3-(4-METHOXYPHENYL)-2-OXAZOLIDINONE

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References

104-94-9 Synthesis

104-94-9
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References