2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE-7-CARBOXYLIC ACID HYDROCHLORIDE synthesis

2synthesis methods

Product Name:2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE-7-CARBOXYLIC ACID HYDROCHLORIDE
CAS Number:149353-83-3
Molecular formula:C11H14ClNO2
Molecular Weight:0

Ethanone, 1-(1,2,4,5-tetrahydro-3H-3-benzazepin-3-yl)-

10533-22-9
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2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE-7-CARBOXYLIC ACID HYDROCHLORIDE

149353-83-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / 1,1-dichloroethane / 2 h / 0 - 20 °C
1.2: 0 °C
2.1: sodium hydroxide; bromine / 1 h / 20 °C
3.1: hydrogenchloride; water / 120 h / Heating / reflux

References:

WO2008/135526,2008,A1

Ethanone, 1-(3-acetyl-2,3,4,5-tetrahydro-1H-3-benzazepin-7-yl)-

149353-98-0
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149353-83-3
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inquiry

References

2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE-7-CARBOXYLIC ACID HYDROCHLORIDE Related Search:

2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE