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ChemicalBook CAS DataBase List 6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER

6-METHYL-BETA-OXO-2-PYRIDINEPROPANOIC ACID ETHYL ESTER synthesis

3synthesis methods
-

Yield:150401-96-0 440 mg

Reaction Conditions:

Stage #1: ethyl acetatewith sodium ethanolate in toluene at 20; for 1 h;Inert atmosphere;
Stage #2: ethyl 6-methylpyridine-2-carboxylate in toluene; for 20 h;Inert atmosphere;Reflux;

References:

WO2013/52613,2013,A1 Location in patent:Paragraph 0160