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Olean-12-en-28-ol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-, (3b)- synthesis

11synthesis methods
Oleana-11,13(18)-dien-28-ol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-, (3β)-

152487-60-0
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Olean-12-en-28-ol, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-, (3b)-

152487-61-1
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Yield:152487-61-1 93%

Reaction Conditions:

with ammonia;lithium in tetrahydrofuran at -78; for 2 h;

References:

Corey;Lee [Journal of the American Chemical Society,1993,vol. 115,# 19,p. 8873 - 8874]