4-BROMOMETHYL-2-METHOXYMETHYL-5-METHYLISOXAZOLIN-3-ONE synthesis
- Product Name:4-BROMOMETHYL-2-METHOXYMETHYL-5-METHYLISOXAZOLIN-3-ONE
- CAS Number:153201-10-6
- Molecular formula:C7H10BrNO3
- Molecular Weight:236.06
110-88-3
228 suppliers
$13.00/100g
67-56-1
738 suppliers
$9.00/25ml
10004-44-1
307 suppliers
$14.14/500mgs:
153201-10-6
14 suppliers
$109.90/5mg
Yield:153201-10-6 16%
Reaction Conditions:
Stage #1: 1,3,5-Trioxan;hymexazolewith sulfuric acid;hydrogen bromide in water at 65; for 12 h;
Stage #2: methanol in dichloromethane at 20; for 2 h;
References:
Asad, Naeem;Deodato, Davide;Dore, Timothy M. [Organic and Biomolecular Chemistry,2021,vol. 19,# 25,p. 5589 - 5594] Location in patent:supporting information