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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER
154187-50-5

2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER synthesis

5synthesis methods
30724-22-2 Synthesis
3'-METHOXY-2,2,2-TRIFLUOROACETOPHENONE

30724-22-2
56 suppliers
$84.00/1g

2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER

154187-50-5
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-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 96 percent / hydroxylamine hydrochloride, pyridine / ethanol / 12 h / 60 °C
2: Et3N, (N,N-dimethylamino)pyridine / CH2Cl2 / 0.75 h / Ambient temperature
3: liq. NH3 / CH2Cl2 / 18 h / Ambient temperature
4: 77 percent / tert-butyl hypochlorite, Et3N / ethanol; 2-methyl-propan-2-ol / 2 h / Ambient temperature
5: 1.) thallium(III) trifluoroacetate, 2.) PdCl2, LiCl, MgO / 1.) TFA, r.t., 24 h, 2.) r.t., 43 h

References:

Hatanaka, Yasumaru;Hashimoto, Makoto;Kurihara, Hiroko;Nakayama, Hitoshi;Kanaoka, Yuichi [Journal of Organic Chemistry,1994,vol. 59,# 2,p. 383 - 387]

Ethanone, 2,2,2-trifluoro-1-(3-methoxyphenyl)-, oxime, (1E)-

140854-00-8
0 suppliers
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2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER

154187-50-5
14 suppliers
inquiry

References
3-(3-METHOXYPHENYL)-3-(TRIFLUOROMETHYL)-DIAZIRIDINE

154187-45-8
17 suppliers
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2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER

154187-50-5
14 suppliers
inquiry

References
Ethanone, 2,2,2-trifluoro-1-(3-methoxyphenyl)-, O-[(4-methylphenyl)sulfonyl]oxime

877667-30-6
0 suppliers
inquiry

2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER

154187-50-5
14 suppliers
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References
67-56-1 Synthesis
Methanol

67-56-1
738 suppliers
$9.00/25ml

201230-82-2 Synthesis
carbon monoxide

201230-82-2
1 suppliers
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3-(3-METHOXYPHENYL)-3-(TRIFLUOROMETHYL)-3H-DIAZIRINE

205485-24-1
25 suppliers
inquiry

2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER

154187-50-5
14 suppliers
inquiry

References

2-METHOXY-4-[3-(TRIFLUOROMETHYL)-3H-DIAZIRIN-3-YL]BENZOIC ACID, METHYL ESTER Related Search:

Benzoic acid, 4-[(1S)-1-aminoethyl]-, methyl ester Benzoic acid, 4-[(1R)-1-aminoethyl]-, methyl ester 4-(1-AZI-2,2,2-TRIFLUOROETHYL)BENZOIC ACID (R)-2,2,2-TRIFLUORO-1-PHENYL-ETHYLAMINE