1,6,7,8-Indolizinetetrol, octahydro-, 1,7,8-triacetate 6-methanesulfonate, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)- synthesis

5synthesis methods

Product Name:1,6,7,8-Indolizinetetrol, octahydro-, 1,7,8-triacetate 6-methanesulfonate, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-
CAS Number:156205-48-0
Molecular formula:C15H23NO9S
Molecular Weight:393.41

79831-76-8 Synthesis

79831-76-8
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1,6,7,8-Indolizinetetrol, octahydro-, 1,7,8-triacetate 6-methanesulfonate, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

156205-48-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 85 percent / pyridine / 0 deg C -> r.t., overnight
2: 30 percent / tributyltin methoxide / tetrahydrofuran / Heating
3: 86 percent / pyridine

References:

Furneaux, Richard H.;Gainsford, Graeme J.;Mason, Jennifer M.;Tyler, Peter C. [Tetrahedron,1994,vol. 50,# 7,p. 2131 - 2160]