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ChemicalBook CAS DataBase List Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI)

Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI) synthesis

6synthesis methods
53308-95-5 Synthesis
BOC-NVA-OH

53308-95-5
231 suppliers
$6.00/1g

Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI)

160801-74-1
7 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: NEt3 / tetrahydrofuran / -10 °C
2: 77 percent / NaBH4 / H2O / 0 °C
3: 92 percent / pyridine-SO3; NEt3; DMSO / CH2Cl2 / -10 °C

References:

Catalano, John G;Deaton, David N;Furfine, Eric S;Hassell, Annie M;McFadyen, Robert B;Miller, Aaron B;Miller, Larry R;Shewchuk, Lisa M;Willard Jr., Derril H;Wright, Lois L [Bioorganic and medicinal chemistry letters,2004,vol. 14,# 1,p. 275 - 278]