ChemicalBook CAS DataBase List Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI)

Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI) synthesis

6synthesis methods

Product Name:Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI)
CAS Number:160801-74-1
Molecular formula:C10H19NO3
Molecular Weight:201.26

53308-95-5 Synthesis

53308-95-5
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$6.00/1g

Carbamic acid, [(1S)-1-formylbutyl]-, 1,1-dimethylethyl ester (9CI)

160801-74-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: NEt₃ / tetrahydrofuran / -10 °C
2: 77 percent / NaBH₄ / H₂O / 0 °C
3: 92 percent / pyridine-SO₃; NEt₃; DMSO / CH₂Cl₂ / -10 °C

References:

Catalano, John G;Deaton, David N;Furfine, Eric S;Hassell, Annie M;McFadyen, Robert B;Miller, Aaron B;Miller, Larry R;Shewchuk, Lisa M;Willard Jr., Derril H;Wright, Lois L [Bioorganic and medicinal chemistry letters,2004,vol. 14,# 1,p. 275 - 278]

carbonyl]butyl]-, 1,1-dimethylethylester

160801-73-0
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160801-74-1
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References

(S)-Methyl 2-((tert-butoxycarbonyl)aMino)pentanoate

64896-37-3
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160801-74-1
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References

24424-99-5 Synthesis

24424-99-5
850 suppliers
$13.50/25G

160801-74-1
7 suppliers
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References

6600-40-4
561 suppliers
$5.00/1g

160801-74-1
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References