1-Pyrrolidinecarboxylic acid, 3-(2-bromo-5-chlorophenoxy)-, 1,1-dimethylethyl ester, (3S)- synthesis

1synthesis methods

Product Name:1-Pyrrolidinecarboxylic acid, 3-(2-bromo-5-chlorophenoxy)-, 1,1-dimethylethyl ester, (3S)-
CAS Number:1609116-53-1
Molecular formula:C15H19BrClNO3
Molecular Weight:376.67

1996-29-8 Synthesis

1996-29-8
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N-(tert-Butoxycarbonyl)-(S)-(+)-3-pyrrolidinol

101469-92-5
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1-Pyrrolidinecarboxylic acid, 3-(2-bromo-5-chlorophenoxy)-, 1,1-dimethylethyl ester, (3S)-

1609116-53-1
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Yield:1609116-53-1 90%

Reaction Conditions:

with potassium tert-butylate in 2-methyltetrahydrofuran;Inert atmosphere;

References:

Murugan, Andiappan;Bachu, Sreekanth;Manjunatha, Sulur G.;Ramakrishnan, Ravi;Kadambar, Vasantha Krishna;Reddy, Chandrasekhara;Torlikonda, Venkata Rao;George, Sajan;Ramasubramanian, Sridharan;Nambiar, Sudhir [Organic Process Research and Development,2014,vol. 18,# 5,p. 646 - 651]