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1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-[(2,4,6-trimethylphenyl)methyl]- synthesis

2synthesis methods
-

Yield:1615227-16-1 84%

Reaction Conditions:

with iron(III)-acetylacetonate;N,N,N,N,-tetramethylethylenediamine;ethylmagnesium bromide in tetrahydrofuran;diethyl ether at 20; for 12 h;Inert atmosphere;

References:

Atack, Thomas C.;Lecker, Rachel M.;Cook, Silas P. [Journal of the American Chemical Society,2014,vol. 136,# 27,p. 9521 - 9523] Location in patent:supporting information