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ChemicalBook CAS DataBase List (3-CYCLOPROPANECARBONYL-PHENYL)-CARBAMIC ACID BENZYL ESTER

(3-CYCLOPROPANECARBONYL-PHENYL)-CARBAMIC ACID BENZYL ESTER synthesis

3synthesis methods
3481-02-5 Synthesis
Cyclopropyl phenyl ketone

3481-02-5
114 suppliers
$14.00/1g

(3-CYCLOPROPANECARBONYL-PHENYL)-CARBAMIC ACID BENZYL ESTER

162174-76-7
12 suppliers
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 50 percent / fuming 90percent nitric acid / 0.17 h / -10 °C
2: hydrogen / 5percent platinum on carbon / methanol / 5 h / 760 Torr
3: diisopropylethylamine / CH2Cl2 / 4 h / Ambient temperature

References:

Thaisrivongs, Suvit;Watenpaugh, Keith D.;Howe, W. Jeffrey;Tomich, Paul K.;Dolak, Lester A.;et al. [Journal of Medicinal Chemistry,1995,vol. 38,# 18,p. 3624 - 3637]

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