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4-Oxazolecarboxylic acid, 4-(4-fluorophenyl)-4,5-dihydro-2-methyl-5-oxo-, ethyl ester synthesis

2synthesis methods
187868-53-7 Synthesis
Propanedioic  acid,  (acetylamino)-,  monoethyl  ester,  (+)-  (9CI)

187868-53-7
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4-Oxazolecarboxylic  acid,  4-(4-fluorophenyl)-4,5-dihydro-2-methyl-5-oxo-,  ethyl  ester

162247-71-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: diethyl ether / 0.25 h / Ambient temperature
2: H2O / diethyl ether / 1 h / Ambient temperature
3: 1.) Pb(OAc)4, Hg(OAc)2, 2.) pyridine / 1.) CHCl3, 40 deg C, 1 h, 2.) 40 deg C, 1 h

References:

Morgan, Jacqueline;Pinhey, John T.;Sherry, Christopher J. [Journal of the Chemical Society. Perkin transactions I,1997,# 5,p. 613 - 619]