Propanedioic acid, 2-amino-2-[2-(4-octylphenyl)ethyl]-, 1,3-diethyl ester synthesis
- Product Name:Propanedioic acid, 2-amino-2-[2-(4-octylphenyl)ethyl]-, 1,3-diethyl ester
- CAS Number:162358-62-5
- Molecular formula:C23H37NO4
- Molecular Weight:391.54
64-17-5
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133826-41-2
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Yield:162358-62-5 54%
Reaction Conditions:
Stage #1: diethyl 2-amino-2-ethylmalonate;4-n-octyliodobenzenewith silver hexafluoroantimonate;2-hydroxy-3-pyridinecarboxaldehyde;palladium diacetate in acetic acid at 20 - 130; for 24.1667 h;Darkness;
Stage #2: ethanolwith thionyl chloride at 0 - 90; for 5 h;
References:
Lin, Hua;Wang, Chao;Bannister, Thomas D.;Kamenecka, Theodore M. [Chemistry - A European Journal,2018,vol. 24,# 38,p. 9535 - 9541] Location in patent:supporting information
102831-44-7
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