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(3-(dibroMoMethylene)-5-(triisopropylsilyl) penta-1,4-diynyl)triMethylsilane synthesis

5synthesis methods
1-(triisopropylsilyl)-5-(triMethylsilyl)-1,4-dipentayne-3-one

167971-40-6
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(3-(dibroMoMethylene)-5-(triisopropylsilyl) penta-1,4-diynyl)triMethylsilane

164990-17-4
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Yield:164990-17-4 93%

Reaction Conditions:

with triphenylphosphine in dichloromethane at 25; for 16 h;

References:

Kohn, Daniel R.;Gawel, Przemyslaw;Xiong, Yaoyao;Christensen, Kirsten E.;Anderson, Harry L. [Journal of Organic Chemistry,2018,vol. 83,# 4,p. 2077 - 2086] Location in patent:supporting information