ChemicalBook CAS DataBase List 3-AMINO-5,6,7,8,9,10-HEXAHYDROCYCLOOCTA[B]THIENO[3,2-E]PYRIDINE-2-CARBOXAMIDE

3-AMINO-5,6,7,8,9,10-HEXAHYDROCYCLOOCTA[B]THIENO[3,2-E]PYRIDINE-2-CARBOXAMIDE synthesis

1synthesis methods

Product Name:3-AMINO-5,6,7,8,9,10-HEXAHYDROCYCLOOCTA[B]THIENO[3,2-E]PYRIDINE-2-CARBOXAMIDE
CAS Number:165066-43-3
Molecular formula:C14H17N3OS
Molecular Weight:275.37

502-49-8 Synthesis

502-49-8
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3-AMINO-5,6,7,8,9,10-HEXAHYDROCYCLOOCTA[B]THIENO[3,2-E]PYRIDINE-2-CARBOXAMIDE

165066-43-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 98 percent / Na, EtOH / diethyl ether
2: 61 percent / acetic acid; ethanol / 3 h / Heating
3: 99 percent / 10percent aq. KOH / dimethylformamide / 0.5 h

References:

Rodinovskaya, L. A.;Belukhina, E. V.;Shestopalov, A. M.;Litvinov, V. P. [Russian Chemical Bulletin,1994,vol. 43,# 3,p. 449 - 457][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1994,# 3,p. 489 - 497]