Phenyl2-azido-2-deoxy-1-thio-beta-D-glucopyranoside synthesis

4synthesis methods

Product Name:Phenyl2-azido-2-deoxy-1-thio-beta-D-glucopyranoside
CAS Number:166516-67-2
Molecular formula:C12H15N3O4S
Molecular Weight:297.33

β-D-Glucopyranoside, phenyl 2-amino-2-deoxy-1-thio-

371123-22-7
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Phenyl2-azido-2-deoxy-1-thio-beta-D-glucopyranoside

166516-67-2
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Yield:166516-67-2 47%

Reaction Conditions:

with dmap;triflic azide in methanol;dichloromethane at 20; for 16 h;

Steps:

1

Example 1According to the following synthetic schemes, glycosyl donor compounds and glycosyl acceptor compounds were prepared, and from the α-anomers obtained by binding the resulting compounds, disaccharide compounds, trisaccharide compounds, and tetrasaccharide compounds were prepared.

References:

US2011/3980,2011,A1 Location in patent:Page/Page column 6-7

β-D-Mannopyranoside, phenyl 2,3:4,6-bis-O-(1-methylethylidene)-1-thio-

151662-55-4
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166516-67-2
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References

108-98-5
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$21.10/10g

166516-67-2
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References

(3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)tetrahydro-2H-pyran-2,4,5-triol hydrochloride

1078691-95-8
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166516-67-2
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References