3-Oxo-4-azaandrosta-1,5,7-triene-17-carboxylic Acid Methyl Ester synthesis
- Product Name:3-Oxo-4-azaandrosta-1,5,7-triene-17-carboxylic Acid Methyl Ester
- CAS Number:166896-63-5
- Molecular formula:C20H25NO3
- Molecular Weight:327.42
103335-41-7
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: lithium trifluoromethanesulfonate / methanol / electrochemical reaction; cathode: stainless steel, anode: carbon felt; constant current of 200 mA
2: 16 h / 100 °C
3: DDQ / CH2Cl2; acetonitrile / -40 °C
4: CH2Cl2; acetonitrile / 18 h / 20 °C
References:
Williams;Marchesini;Reamer;Dolling;Grabowski [Journal of Organic Chemistry,1995,vol. 60,# 16,p. 5337 - 5340]
166896-62-4
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1026013-15-9
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