![](/CAS/20180808/GIF/168163-93-7.gif)
4-fluoro-1-tosyl-3,4-dihydro-1H-benzo[b]azepin-5(2H)-one(WXC02963) synthesis
- Product Name:4-fluoro-1-tosyl-3,4-dihydro-1H-benzo[b]azepin-5(2H)-one(WXC02963)
- CAS Number:168163-93-7
- Molecular formula:C17H16FNO3S
- Molecular Weight:333.38
![1-(TOLUENE-4-SULFONYL)-1,2,3,4-TETRAHYDROBENZO[B]AZEPIN-5-ONE](/CAS/GIF/24310-36-9.gif)
24310-36-9
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$28.60/25mg
![4-fluoro-1-tosyl-3,4-dihydro-1H-benzo[b]azepin-5(2H)-one(WXC02963)](/CAS/20180808/GIF/168163-93-7.gif)
168163-93-7
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Yield:168163-93-7 78%
Reaction Conditions:
Stage #1: 1-tosyl-2,3,4,5-tetrahydro-1H-1-benzazepin-5-onewith lithium diisopropyl amide in tetrahydrofuran at -78; for 0.5 h;
Stage #2: with N-fluorobis(benzenesulfon)imide in tetrahydrofuran at 0; for 1 h;
References:
Shimada;Taniguchi;Matsuhisa;Sakamoto;Yatsu;Tanaka [Chemical and Pharmaceutical Bulletin,2000,vol. 48,# 11,p. 1644 - 1651]