ChemicalBook CAS DataBase List 17-IODOHEPTADECANOIC ACID

17-IODOHEPTADECANOIC ACID synthesis

9synthesis methods

Product Name:17-IODOHEPTADECANOIC ACID
CAS Number:60451-92-5
Molecular formula:C17H33IO2
Molecular Weight:396.35

30515-28-7 Synthesis

30515-28-7
165 suppliers
$7.00/250mg

60451-92-5
22 suppliers
$160.00/100mg

Yield:-

Steps:

Multi-step reaction with 7 steps
1: NH₃ / tetrahydrofuran / 15 h
2: diethyl ether
3: LiAlH₄ / diethyl ether / 2 h / 0 °C
4: 54 percent / LiNH₂, Fe(NO₃)3 / tetrahydrofuran; NH₃ / 20 h
5: H₂ / PtO₂ / diethyl ether
6: pyridine / 0 °C
7: NaI / acetone / 2 h / Heating

References:

Riche, Francoise;Mathieu, Jean-Paul;Vincens, Maurice;Bardy, Andre;Comet, Michel;Vidal, Michel [Bulletin de la Societe Chimique de France,1984,vol. 2,# 1-2,p. 49 - 55]

30964-01-3 Synthesis