ChemicalBook CAS DataBase List Methyl 6-((tert-butoxycarbonyl)aMino)spiro[3.3]heptane-2-carboxylate

Methyl 6-((tert-butoxycarbonyl)aMino)spiro[3.3]heptane-2-carboxylate synthesis

2synthesis methods

Product Name:Methyl 6-((tert-butoxycarbonyl)aMino)spiro[3.3]heptane-2-carboxylate
CAS Number:170508-14-2
Molecular formula:C14H23NO4
Molecular Weight:269.34

spiro[3.3]heptane-2,6-dicarboxylic acid monomethyl ester

10481-25-1
55 suppliers
$200.00/100mg

Methyl 6-((tert-butoxycarbonyl)aMino)spiro[3.3]heptane-2-carboxylate

170508-14-2
52 suppliers
$21.00/100mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) i-BuOCOCl, NEt₃, 2.) NH₃ / 1.) THF, 0 deg C, 40 min, 2.) 0 deg C, 30 min; room temperature, 1 h
2: 62 percent / Pb(OAc)4 / dimethylformamide / 0.67 h / Heating

References:

Jones;Drach;Corbett;Kessel;Zemlicka [Journal of Organic Chemistry,1995,vol. 60,# 20,p. 6277 - 6280]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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75-65-0 Synthesis

75-65-0
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170508-14-2
52 suppliers
$21.00/100mg

References