Propanoic acid, 2,2-dimethyl-, octahydro-1,6,7-tris(phenylmethoxy)-8-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)- synthesis

2synthesis methods

Product Name:Propanoic acid, 2,2-dimethyl-, octahydro-1,6,7-tris(phenylmethoxy)-8-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-
CAS Number:171925-40-9
Molecular formula:
Molecular Weight:0

79831-76-8 Synthesis

79831-76-8
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$33.00/5mg

Propanoic acid, 2,2-dimethyl-, octahydro-1,6,7-tris(phenylmethoxy)-8-indolizinyl ester, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

171925-40-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.)Bu₂SnO, 2.) Bu₄NBr, 3.) LiH, Pr-SH / 1.) MePh, reflux, 2 h, 2.) MePh, reflux, 3 days, 3.) DMSO, 3 h
2: 63 percent / pyridine / 30 h / 70 °C

References:

Furneaux, Richard H.;Gainsford, Graeme J.;Mason, Jennifer M.;Tyler, Peter C.;Hartley, Oliver;Winchester, Bryan G. [Tetrahedron,1995,vol. 51,# 46,p. 12611 - 12630]

3282-30-2
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8-Indolizinol, octahydro-1,6,7-tris(phenylmethoxy)-, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-

156150-89-9
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171925-40-9
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References