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ChemicalBook CAS DataBase List METHYL 5,7,8,9-TETRA-O-ACETYL-4-ACYLAMINO-2,6-ANHYDRO-3,4-DIDEOXY-D-GLYCERO-D-GALACTO-2-ENONATE

METHYL 5,7,8,9-TETRA-O-ACETYL-4-ACYLAMINO-2,6-ANHYDRO-3,4-DIDEOXY-D-GLYCERO-D-GALACTO-2-ENONATE synthesis

4synthesis methods
D-glycero-β-D-galacto-2-Nonulopyranosonic acid, 3-deoxy-, methyl ester, 2,4,5,7,8,9-hexaacetate

123843-50-5
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2-Furancarboxylic acid, 5-[(1S,2R,3R)-1,2,3,4-tetrakis(acetyloxy)butyl]-, methyl ester

173467-17-9
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D-glycero-D-talo-Non-2-enonic acid, 4-(acetylamino)-2,6-anhydro-3,4-dideoxy-, methyl ester, 5,7,8,9-tetraacetate

173467-19-1
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METHYL 5,7,8,9-TETRA-O-ACETYL-4-ACYLAMINO-2,6-ANHYDRO-3,4-DIDEOXY-D-GLYCERO-D-GALACTO-2-ENONATE

173467-18-0
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Yield:173467-18-0 16% ,173467-19-1 70% ,173467-17-9 9%

Reaction Conditions:

with trimethylsilyl trifluoromethanesulfonate in acetonitrile; for 3 h;Ambient temperature;

References:

Sun;Kai;Tanaka;Takayanagi;Furuhata [Chemical and Pharmaceutical Bulletin,1995,vol. 43,# 10,p. 1654 - 1658]