2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]-5-NITROBENZONITRILE synthesis

1synthesis methods

Product Name:2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]-5-NITROBENZONITRILE
CAS Number:175135-68-9
Molecular formula:C9H5N5O2S2
Molecular Weight:279.3

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2349-67-9 Synthesis

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2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]-5-NITROBENZONITRILE

175135-68-9
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Yield:175135-68-9 67%

Reaction Conditions:

Stage #1: 2-Amino-5-mercapto-1,3,4-thiadiazolewith potassium carbonate in acetone; for 0.5 h;
Stage #2: 4-chloro-3-cyanonitrobenzene in acetone; for 2 h;Reflux;

References:

Chen, Yong-Fei;Ni, Nanting;Li, Minyong;Xu, Peng-Fei;Wang, Binghe [Heterocyclic Communications,2010,vol. 16,# 2-3,p. 123 - 135] Location in patent:experimental part

2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]-5-NITROBENZONITRILE Related Search:

5-Amino-1,3,4-thiadiazole-2-thiol 2-(Methylthio)-5-nitrobenzonitrile 2-Amino-1,3,4-thiadiazole 2-Mercapto-1,3,4-thiadiazol 2-AMINO-5-(METHYLTHIO)-1,3,4-THIADIAZOLE