ChemicalBook CAS DataBase List Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R-

Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R- synthesis

1synthesis methods

Product Name:Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R-
CAS Number:177472-54-7
Molecular formula:C9H17NO3
Molecular Weight:187.24

Cyclopropanecarboxylic acid, 2-[bis[(1,1-dimethylethoxy)carbonyl]amino]-, ethyl ester, (1R,2R)-

1421676-97-2
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Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R-

177472-54-7
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Yield:177472-54-7 60%

Reaction Conditions:

with diisobutylaluminium hydride in toluene at -78; for 4 h;Inert atmosphere;enantioselective reaction;

References:

Chanthamath, Soda;Nguyen, Dao Thi;Shibatomi, Kazutaka;Iwasa, Seiji [Organic Letters,2013,vol. 15,# 4,p. 772 - 775] Location in patent:supporting information