![](/CAS/20210111/GIF/177472-54-7.gif)
Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R- synthesis
- Product Name:Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R-
- CAS Number:177472-54-7
- Molecular formula:C9H17NO3
- Molecular Weight:187.24
![Cyclopropanecarboxylic acid, 2-[bis[(1,1-dimethylethoxy)carbonyl]amino]-, ethyl ester, (1R,2R)-](/CAS/20210305/GIF/1421676-97-2.gif)
1421676-97-2
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![Carbamic acid, [2-(hydroxymethyl)cyclopropyl]-, 1,1-dimethylethyl ester, (1R-](/CAS/20210111/GIF/177472-54-7.gif)
177472-54-7
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Yield:177472-54-7 60%
Reaction Conditions:
with diisobutylaluminium hydride in toluene at -78; for 4 h;Inert atmosphere;enantioselective reaction;
References:
Chanthamath, Soda;Nguyen, Dao Thi;Shibatomi, Kazutaka;Iwasa, Seiji [Organic Letters,2013,vol. 15,# 4,p. 772 - 775] Location in patent:supporting information