(R,E)-2-(benzo[d][1,3]dioxol-5-ylMethyleneaMino)-2-phenylethanol synthesis
2synthesis methods
- Product Name:(R,E)-2-(benzo[d][1,3]dioxol-5-ylMethyleneaMino)-2-phenylethanol
- CAS Number:179930-11-1
- Molecular formula:C16H15NO3
- Molecular Weight:269.3
Yield:179930-11-1 95.4%
Reaction Conditions:
with toluene-4-sulfonic acid in toluene;Reflux;Dean-Stark;Large scale;
References:
Storace, Louis;Anzalone, Luigi;Confalone, Pat N.;Davis, Wayne P.;Fortunak, Joseph M.;Giangiordano, Mark;Haley Jr., James J.;Kamholz, Kenneth;Li, Hui-Yin;Ma, Philip;Nugent, William A.;Parsons Jr., Rodney L.;Sheeran, Patrick J.;Silverman, Charlotte E.;Waltermire, Robert E.;Wood, Christopher C. [Organic Process Research and Development,2002,vol. 6,# 1,p. 54 - 63]
