3-(diMethylaMino)-1-(4-Methoxyphenyl)prop-2-en-1-one synthesis
- Product Name:3-(diMethylaMino)-1-(4-Methoxyphenyl)prop-2-en-1-one
- CAS Number:18096-70-3
- Molecular formula:C12H15NO2
- Molecular Weight:205.25
4637-24-5
589 suppliers
$5.00/25g
100-06-1
580 suppliers
$22.10/25g
18096-70-3
30 suppliers
$45.00/100mg
Yield:18096-70-3 100%
Reaction Conditions:
in N,N-dimethyl-formamide; for 3.5 h;Reflux;
Steps:
Preparation of 3-dimethylamino-1-(4-methoxyphenyl)-2-propene-1-one:
Dissolve p-methoxyacetophenone (150mg, 1.0mmol) and N,N-dimethylformamide dimethyl acetal (DMFDMA) (476mg, 4.0mmol) in about 5.0ml of DMF, and heat to reflux 3.5 hours, TLC detects that the raw material is almost completely reacted. The reaction solution was concentrated to obtain 205 mg of yellow solid with a yield of 100%.
References:
CN111925368,2020,A Location in patent:Paragraph 0169-0174
20353-93-9
48 suppliers
$22.39/1G
100-06-1
580 suppliers
$22.10/25g
18096-70-3
30 suppliers
$45.00/100mg
1188-33-6
246 suppliers
$11.19/5ML
100-06-1
580 suppliers
$22.10/25g
18096-70-3
30 suppliers
$45.00/100mg