Hydrazinecarboxylic acid, 2-(1-ethylpropyl)-, 1,1-dimethylethyl ester (9CI) synthesis

3synthesis methods

Product Name:Hydrazinecarboxylic acid, 2-(1-ethylpropyl)-, 1,1-dimethylethyl ester (9CI)
CAS Number:184177-78-4
Molecular formula:C10H22N2O2
Molecular Weight:202.2939

870-46-2 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 92 percent / toluene / 1 h / 50 °C
2: 61 percent / DIBAL / tetrahydrofuran; toluene / 4 h / -78 - -40 °C

References:

Bailey, Murray D.;Halmos, Ted;Goudreau, Nathalie;Lescop, Ewen;Llinàs-Brunet, Montse [Journal of Medicinal Chemistry,2004,vol. 47,# 15,p. 3788 - 3799]

184177-77-3 Synthesis