7-Oxabicyclo[2.2.1]hept-5-ene-2-carboxylicacid,methylester,(1S,2S,4S)- synthesis

3synthesis methods

Product Name:7-Oxabicyclo[2.2.1]hept-5-ene-2-carboxylicacid,methylester,(1S,2S,4S)-
CAS Number:186766-46-1
Molecular formula:C8H10O3
Molecular Weight:154.16

67-56-1 Synthesis

67-56-1
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7-Oxabicyclo[2.2.1]hept-5-ene-2-carbothioic acid, S-ethyl ester, (1S,2S,4S)-

245680-45-9
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7-Oxabicyclo[2.2.1]hept-5-ene-2-carboxylicacid,methylester,(1S,2S,4S)-

186766-46-1
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Yield:186766-46-1 93%

Reaction Conditions:

with caesium carbonate at 0;transesterification;

References:

Evans, David A.;Barnes, David M.;Johnson, Jeffrey S.;Lectka, Thomas;Von Matt, Peter;Miller, Scott J.;Murry, Jerry A.;Norcross, Roger D.;Shaughnessy, Eileen A.;Campos, Kevin R. [Journal of the American Chemical Society,1999,vol. 121,# 33,p. 7582 - 7594]

2-Oxazolidinone, 3-[(1S,2S,4S)-7-oxabicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-

186666-50-2
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186766-46-1
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References

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186766-46-1
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References