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Carbamic acid, (1-formylethenyl)-, 1,1-dimethylethyl ester (9CI) synthesis

6synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
825 suppliers
$13.50/25G

Carbamic acid, (1-formylethenyl)-, 1,1-dimethylethyl ester (9CI)

186795-56-2
4 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 90 percent / methanol / 4 h / Ambient temperature
2: 25 percent / pyridine sulfur trioxide, DMSO, Et3N / 0.5 h / Ambient temperature

References:

Harada, Hiroshi;Morie, Toshiya;Hirokawa, Yoshimi;Kato, Shiro [Chemical and Pharmaceutical Bulletin,1996,vol. 44,# 12,p. 2205 - 2212]