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19-HYDROXYCHOLESTENONE synthesis

5synthesis methods
Cholest-4-en-3-one, 19-[[2-(acetylamino)-2-deoxy-β-D-glucopyranosyl]oxy]-

1261029-94-0
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19-HYDROXYCHOLESTENONE

13200-77-6
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Yield:13200-77-6 56%

Reaction Conditions:

with pyridinium p-toluenesulfonate in benzene at 90; for 3.5 h;

References:

Lin, An-Shen;Engel, Sebastian;Smith, Benjamin A.;Fairchild, Craig R.;Aalbersberg, William;Hay, Mark E.;Kubanek, Julia [Bioorganic and Medicinal Chemistry,2010,vol. 18,# 23,p. 8264 - 8269] Location in patent:experimental part

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