Benzoic acid, 4-(trifluoromethyl)-, 1,1-dimethylethyl ester synthesis

10synthesis methods

Product Name:Benzoic acid, 4-(trifluoromethyl)-, 1,1-dimethylethyl ester
CAS Number:196934-20-0
Molecular formula:C12H13F3O2
Molecular Weight:246.23

455-14-1
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201230-82-2 Synthesis

201230-82-2
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75-65-0 Synthesis

75-65-0
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Benzoic acid, 4-(trifluoromethyl)-, 1,1-dimethylethyl ester

196934-20-0
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Yield:196934-20-0 110.8 mg

Reaction Conditions:

Stage #1: 4-trifluoromethylphenylaminewith tetrafluoroboric acid;sodium nitrite in water at 0; for 0.75 h;
Stage #2: carbon monoxide;tert-butyl alcoholwith sodium formate in acetonitrile at 20; under 37503.8 Torr; for 3 h;

References:

Koziakov, Denis;Jacobi Von Wangelin, Axel [Organic and Biomolecular Chemistry,2017,vol. 15,# 32,p. 6715 - 6719] Location in patent:supporting information

201230-82-2 Synthesis

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402-43-7 Synthesis