1H-Benzimidazole,2-(2,2,2-trifluoroethyl)-(9CI) synthesis
2synthesis methods
- Product Name:1H-Benzimidazole,2-(2,2,2-trifluoroethyl)-(9CI)
- CAS Number:105942-28-7
- Molecular formula:C9H7F3N2
- Molecular Weight:200.16
Yield:105942-28-7 81%
Reaction Conditions:
with 2,2'-azobis-(2,4-dimethylvaleronitrile);sodium hydrogencarbonate;sulfur;bis(pinacol)diborane in N,N-dimethyl-formamide at 100; for 15 h;Inert atmosphere;
References:
Li, Zhengyu;Dong, Jingnan;Wang, Junwen;Yang, Ding-Yah;Weng, Zhiqiang [Chemical Communications,2019,vol. 55,# 87,p. 13132 - 13135] Location in patent:supporting information
