1H-Indazol-3-amine, 1-(phenylmethyl)- synthesis
- Product Name:1H-Indazol-3-amine, 1-(phenylmethyl)-
- CAS Number:28519-78-0
- Molecular formula:C14H13N3
- Molecular Weight:223.27
185011-16-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: H2 / 2 percent Pd/C / methanol / 8 h / 40 - 45 °C
2.1: 0.2 g / methanol / 3 h / Heating
3.1: 99 percent / aq. HCl / 0.25 h / Heating
4.1: KOH / dimethylsulfoxide / 0.08 h
4.2: 70 percent / dimethylsulfoxide / 2 h / 20 °C
References:
Dyablo;Pozharskii;Kuz'menko;Kolesnichenko [Chemistry of Heterocyclic Compounds,2001,vol. 37,# 5,p. 567 - 573]
185011-20-5
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28519-78-0
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2042-37-7
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$7.00/10g
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