1H-Isoindole-1,3(2H)-dione, 5-iodo- synthesis
- Product Name:1H-Isoindole-1,3(2H)-dione, 5-iodo-
- CAS Number:98556-60-6
- Molecular formula:C8H4INO2
- Molecular Weight:273.03
511533-38-3
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Yield:98556-60-6 99%
Reaction Conditions:
with manganese(IV) oxide;ammonium hydroxide;oxygen;chlorobenzene in N,N-dimethyl-formamide at 100; under 15001.5 Torr; for 24 h;Autoclave;Green chemistry;
Steps:
6; 35 Example 35:
General procedure: 0.01g of MnO2 catalyst, 0.5mmol of 1-indanone, 0.2g of ammonia water (25wt%) and 2g of chlorobenzene were added to a stainless steel autoclave with a polytetrafluoroethylene inner liner.The temperature was raised to 110 by automatic temperature controller, 0.6MPa oxygen was added and the reaction was continued for 4h. The pressure was kept constant during the reaction.The reaction product was analyzed using GC-MS with a phthalamide yield of 85%.
References:
CN106278990,2017,A Location in patent:Paragraph 0013; 0017; 0018; 0020; 0024; 0028
3676-85-5
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