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1H-Pyrrolo[3,2-c]pyridine-2,3-dione(9CI) synthesis

2synthesis methods
98400-69-2 Synthesis
4-(Boc-amino)pyridine

98400-69-2
172 suppliers
$6.00/1g

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) tBuLi / 1.) THF, hexane, -10 deg C, 3 h, 2.) THF, hexane, a) -78 deg C, 5 min, b) RT, 15 min
2: 68 percent / 0.42 h / 192 °C

References:

Rivalle, Christian;Bisagni, Emile [Journal of Heterocyclic Chemistry,1997,vol. 34,# 2,p. 441 - 444]