ChemicalBook CAS DataBase List (1S,3S)-3-AMINOCYCLOHEXANOL

(1S,3S)-3-AMINOCYCLOHEXANOL synthesis

3synthesis methods

Product Name:(1S,3S)-3-AMINOCYCLOHEXANOL
CAS Number:721884-81-7
Molecular formula:C6H13NO
Molecular Weight:115.17

6850-39-1
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721884-81-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 17 percent / NaOH / H₂O / 3 h / 20 °C
2.1: 75 percent / Et₃N / tetrahydrofuran
3.1: Novozyme(R) 435 from Candida antarctica B / ethanol; toluene / 120 h / 18 - 22 °C
3.2: LiAlH₄ / tetrahydrofuran / 72 h / Heating
3.3: H₂ / Pd/C / ethanol / 16 h / 760 Torr

References:

Bernardelli, Patrick;Bladon, Michael;Lorthiois, Edwige;Manage, Ajith C.;Vergne, Fabrice;Wrigglesworth, Roger [Tetrahedron Asymmetry,2004,vol. 15,# 9,p. 1451 - 1455]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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721884-81-7
40 suppliers
$193.00/50mg

References

13941-94-1
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721884-81-7
40 suppliers
$193.00/50mg

References