2-(1,1,2,2-TETRAFLUOROETHOXY)TOLUENE synthesis
1synthesis methods
- Product Name:2-(1,1,2,2-TETRAFLUOROETHOXY)TOLUENE
- CAS Number:42145-66-4
- Molecular formula:C9H8F4O
- Molecular Weight:208.15
Yield: 82%
Reaction Conditions:
Stage #1:1,2-dibromo-1,1,2,2-tetrafluoroethane;ortho-cresol with caesium carbonate in dimethyl sulfoxide at 50; for 5 h;
Stage #2: with acidic acid;zinc at 50; for 1 h;Further stages.;
References:
Li, Jianqing;Qiao, Jennifer X.;Smith, Daniel;Chen, Bang-Chi;Salvati, Mark E.;Roberge, Jacques Y.;Balasubramanian, Balu N. [Tetrahedron Letters,2007,vol. 48,# 42,p. 7516 - 7519]