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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2-(1,3-dioxolan-2-yl)Benzaldehyde synthesis

5synthesis methods
2-Bromobenzaldehyde

6630-33-7
406 suppliers
$9.00/10g

2-(1,3-dioxolan-2-yl)Benzaldehyde

59259-01-7
3 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid / toluene / 18 h / Reflux; Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / -78 - -30 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere

References:

Che, Chao;Li, Song;Yu, Zhixiong;Li, Fangfang;Xin, Shengchang;Zhou, Liyan;Lin, Shuo;Yang, Zhen [ACS Combinatorial Science,2013,vol. 15,# 4,p. 202 - 207]

Benzenemethanol, 2-(1,3-dioxolan-2-yl)-

23691-82-9
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2-(1,3-dioxolan-2-yl)Benzaldehyde

59259-01-7
3 suppliers
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References
2591-86-8 Synthesis
N-Formylpiperidine

2591-86-8
294 suppliers
$14.00/5g

34824-58-3 Synthesis
2-(2-BROMOPHENYL)-1,3-DIOXOLANE

34824-58-3
141 suppliers
$9.00/1g

2-(1,3-dioxolan-2-yl)Benzaldehyde

59259-01-7
3 suppliers
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References
1708-41-4 Synthesis
2-(1,3-DIOXOLAN-2-YL)FURAN

1708-41-4
46 suppliers
$45.00/250mg

Acrolein

107-02-8
4 suppliers
$38.60/4s8501

2-(1,3-dioxolan-2-yl)Benzaldehyde

59259-01-7
3 suppliers
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3-(1,3-dioxolan-2-yl)Benzaldehyde

68348-23-2
10 suppliers
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References
107-21-1 Synthesis
Ethylene glycol

107-21-1
1315 suppliers
$10.00/25g

643-79-8 Synthesis
o-Phthalaldehyde

643-79-8
697 suppliers
$9.00/1g

2-(1,3-dioxolan-2-yl)Benzaldehyde

59259-01-7
3 suppliers
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References