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2-(2,3-DICHLORO-PHENYL)-BENZOOXAZOL-5-YLAMINE synthesis
1synthesis methods
- Product Name:2-(2,3-DICHLORO-PHENYL)-BENZOOXAZOL-5-YLAMINE
- CAS Number:339197-79-4
- Molecular formula:C13H8Cl2N2O
- Molecular Weight:279.12
Yield:339197-79-4 83%
Reaction Conditions:
with polyphosphoric acid at 110 - 120; for 16 h;
References:
Chancellor, Daniel R.;Davies, Kay E.;De Moor, Olivier;Dorgan, Colin R.;Johnson, Peter D.;Lambert, Adam G.;Lawrence, Daniel;Lecci, Cristina;Maillol, Carole;Middleton, Penny J.;Nugent, Gary;Poignant, Séverine D.;Potter, Allyson C.;Price, Paul D.;Pye, Richard J.;Storer, Richard;Tinsley, Jonathon M.;Van Well, Renate;Vickers, Richard;Vile, Julia;Wilkes, Fraser J.;Wilson, Francis X.;Wren, Stephen P.;Wynne, Graham M. [Journal of Medicinal Chemistry,2011,vol. 54,# 9,p. 3241 - 3250] Location in patent:supporting information; experimental part