2,2,3-trimethylbutan-1-ol synthesis

13synthesis methods

Product Name:2,2,3-trimethylbutan-1-ol
CAS Number:55505-23-2
Molecular formula:C7H16O
Molecular Weight:116.2013

126-30-7 Synthesis

126-30-7
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55505-23-2
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 1.5 h / 0 °C / Inert atmosphere
1.2: Cooling with ice; Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 20 °C / Cooling with acetone-dry ice; Inert atmosphere
2.2: 0 - 20 °C

References:

Elliott, Mark C.;Smith, Keith;Heulyn Jones;Hussain, Ajaz;Saleh, Basil A. [Journal of Organic Chemistry,2013,vol. 78,# 7,p. 3057 - 3064]

Butanoic acid, 2,2,3-trimethyl-, ethyl ester

1727-61-3
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55505-23-2
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References

1,3,2-Dioxaborolane, 2-(1,1,2-trimethylpropyl)-

99810-77-2
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74-95-3 Synthesis

74-95-3
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594-60-5
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55505-23-2
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References

Boronic acid, B-(1,1,2-trimethylpropyl)-, dimethyl ester

56118-62-8
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74-95-3 Synthesis

74-95-3
259 suppliers
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594-60-5
40 suppliers
$143.00/5g

55505-23-2
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References

1,3,2-Dioxaborinane, 2-(1,1,2-trimethylpropyl)-

63689-74-7
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74-95-3 Synthesis

74-95-3
259 suppliers
$10.00/10g

594-60-5
40 suppliers
$143.00/5g

55505-23-2
4 suppliers
inquiry

References