![32403-69-3](/StructureFile/ChemBookStructure3/GIF/CB3347423.gif)
2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID synthesis
- Product Name:2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID
- CAS Number:32403-69-3
- Molecular formula:C8H6N2O6S
- Molecular Weight:258.21
Yield:32403-69-3 74%
Reaction Conditions:
with triethylamine in 1,4-dioxane;water;
Steps:
7 2-(2,4-Dinitrophenylthio)-acetic acid
Example 7 2-(2,4-Dinitrophenylthio)-acetic acid Et3N (1.5 g, 15 mmol) and mercapto-acetic acid (1 g, 11 mmol) were added to a solution of 1-chloro-2,4-dinitrobenzene (2.26 g, 10 mmol) in 1,4-dioxane (50 mL) at room temperature. After stirring at room temperature for 5 h, H2O (100 mL) was added. The resulting suspension was extracted with ethyl acetate (100 mL*3). The ethyl acetate extract was washed with water and brine, dried over Na2SO4 and concentrated to give 2-(2,4-dinitrophenylthio)-acetic acid (2.3 g, 74%), which was used without further purification.
References:
US2011/98311,2011,A1 US2012/309758,2012,A1
![Benzenesulfonic acid, 2,4-dinitro-, 2-(2-benzothiazolyl)phenyl ester](/CAS/20210305/GIF/1373156-67-2.gif)
1373156-67-2
0 suppliers
inquiry
![Thioglycolic acid](/CAS/GIF/68-11-1.gif)
68-11-1
417 suppliers
$12.00/25g
![2-(2-Hydroxyphenyl)benzothiazole](/CAS/GIF/3411-95-8.gif)
3411-95-8
215 suppliers
$5.00/250mg
![2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID](/StructureFile/ChemBookStructure3/GIF/CB3347423.gif)
32403-69-3
12 suppliers
inquiry
![BIS(2,4-DINITROPHENYL) DISULFIDE](/CAS/GIF/2217-55-2.gif)
2217-55-2
29 suppliers
$156.00/25g
![2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID](/StructureFile/ChemBookStructure3/GIF/CB3347423.gif)
32403-69-3
12 suppliers
inquiry
![2,4-Dinitrochlorobenzene](/CAS/GIF/97-00-7.gif)
97-00-7
12 suppliers
$17.67/10gm:
![2-(2,4-DINITRO PHENYLTHIO) ACETIC ACID](/StructureFile/ChemBookStructure3/GIF/CB3347423.gif)
32403-69-3
12 suppliers
inquiry